辐照用小尺寸样品力学性能表征技术研究进展

由于辐照空间尺寸限制、降低样品放射性和提高辐照参数精度等原因，小尺寸样品被广泛应用于核反应堆材料的辐照后力学性能表征。本文就国内外小尺寸拉伸、冲击、断裂韧性、疲劳、蠕变和小冲杆等测试表征技术的研究现状进行了综合论述，分析了小尺寸样品测试中的关键影响因素以及数据归一化方法，总结了小尺寸样品存在的问题，并结合我国需求对小尺寸样品技术的发展进行了分析和展望，以期为小尺寸样品技术及测试分析数据进一步规范化和工程应用发展提供参考。     

Dependence of grip strength on shoulder position and its implications for ergonomics practice

Grip strength (GS) variability due to positional changes in the upper extremity joints is of importance while designing workstations and work methods. This study was conducted to analyze the GS variations due to positional changes at shoulder joint when some important variables were under control. The GSs of dominant and nondominant hands were measured in eight shoulder (0°, 45°, 90°, and 135° of flexion and abduction) and standard test positions (STP). One hundred and thirteen subjects 20–30 years old completed the study. At the dominant side, no significant difference was observed in the pairwise comparisons between STP and the others. Maximum and minimum GSs were obtained in 0° abduction and 45° flexion and abduction, respectively. At the nondominant side, GSs were significantly lower (p < 0.001) in the corresponding test positions and demonstrated more variability. The findings of this study can contribute to the available knowledge to guide occupational ergonomists in their practices.     

Influence of temperature cycling and pore fluid on tensile strength of chalk

Calcite has a highly anisotropic thermal expansion coefficient, and repeated heating and cooling cycles can potentially destabilize chalks by breaking cement bonds between neighboring particles. Based on tensile strength measurements, we investigated how temperature cycles induce weakening of chalk. Tensile strength tests were performed on chalk specimens sampled from Kansas (USA) and Mons (Belgium), each with differing amounts of contact cement. Samples of the two chalk types were tested in dry and water-saturated states, and then exposed to 0, 15, and 30 temperature cycles in order to find out under what circumstances thermally induced tensile strength reduction occurs. The testing results show that the dry samples were not influenced by temperature cycling in either of the chalk types. However, in the water-saturated state, tensile strength is increasingly reduced with progressive numbers of temperature cycles for both chalk samples, especially for the more cemented Kansas chalk. The Kansas chalk demonstrated higher initial tensile strength compared to the less cemented Mons chalk, but the strength of both chalks was reduced by the same relative proportion when undergoing thermal cycles in the water-saturated state.     

Alginate–chitosan composite hydrogel film with macrovoids in the inner layer for biomedical applications

Making of a layered composite using two biopolymer gels with regularly aligned voids in the inner layer is described in this article. Calcium alginate constituted the inner layer, within which voids of 500 μm diameter were embedded in monolayer or in multiple layers using a fluidic device for bubbling. The chitosan without any additional crosslinker was used to form the outer layer. The layered structure enabled compartmentalization of drug hold-up, and differential release rates. These aspects were reviewed using bovine serum albumin and vitamin B₁₂ as model solutes. The presence of voids at the inner layer of alginate increased the uptake, raising the level of absorptivity to more than 4000%. The composite film could hold two solutes at a time. The one, held inside the alginate layer started releasing only after 1 h of dipping in the release media. The adhesive strength between layers and the response of the composite film to compressive deformation are studied here. The effect of single or multiple layers of voids in the inner layer is reviewed. The slowing of degradation rate due to chitosan-encapsulation is experimentally determined. © 2019 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2019 , 136, 47599.     

A new cladding technology to bond aluminium on magnesium

ABSTRACT

An in situ hot press bonding technology has been developed to clad aluminium on magnesium. Followed by regular hot rolling, magnesium sheets, covered by ductile and corrosion-resistant aluminium without detectable oxides in the interface, are produced. The new technology requires no welding, vacuum, protective atmosphere or barrier layer, and it makes good interfacial strength and rollability. Aluminium–magnesium intermetallic phases are formed along the clad–core interface at elevated temperatures. They are not detrimental under compression but may cause clad-core delamination in tensile strain. However, the tensile failure is more dependent on the formability of magnesium core than on the strength of interface.     

300M超高强钢在中性盐雾环境中的腐蚀行为及机制

摘要：为了研究300M超高强钢在中性盐雾环境中的腐蚀行为及腐蚀机制，采用失重法，宏观、微观腐蚀形貌分析，三维表面轮廓分析及电化学分析的研究方法，来表征腐蚀实验现象并进行分析。结果表明：300M超高强钢在中性盐雾环境中的腐蚀产物为FeOOH、Fe2O3、Fe(OH)3和Fe3O4；腐蚀速率随着腐蚀时间逐渐降低，腐蚀后期（72h）腐蚀速率降低50%；腐蚀初期以点蚀为主，点蚀坑通过横向扩展，逐渐发展为后期的均匀腐蚀，腐蚀表面形貌呈沟壑状；外腐蚀层对基体的保护能力很弱，Cr元素在锈层靠近基体的一侧偏聚使内腐蚀层具有一定的抗腐蚀性。     

钴/镍复合中间层真空扩散连接钨与钢

以钴粉/镍箔为复合中间层，采用800，900和1 000 ℃等三种连接温度，加压10 MPa并保温120 min的工艺条件，对钨/钢真空扩散连接. 研究了接头的微观组织、成分分布、力学性能及断口特征. 结果表明，连接温度为800 ℃和900 ℃时，钨/中间层界面金属间化合物生成很少，对应接头抗剪强度分别为186 MPa和172 MPa，断口均位于钨母材中近界面的位置，为典型解理断裂形貌；当连接温度升至1 000 ℃时，钨/中间层界面生成厚度小于2 μm的连续金属间化合物层，接头抗剪强度降至115 MPa，断裂也发生在钨母材中近界面的位置，断口大部分区域为沿晶断裂特征.     

Co/Al金属在聚晶立方氮化硼中的作用及加工适用性

通过正交试验和切削试验相结合的方法,检测聚晶立方氮化硼(PCBN)烧结体的硬度和强度,分析并观察烧结体组元相互熔渗状况以及微观形貌,探索了Co/Al金属对PCBN烧结体的影响以及不同结合剂含量PCBN的加工适应性。试验结果表明:CBN含量和Co含量对PCBN的抗弯强度和硬度影响显著;在刀具材料的选择上,高PCBN浓度的刀具适合加工灰铸铁,低PCBN浓度的刀具适合加工淬硬钢;Co/Al金属能够通过高温高压在PCBN层和硬质合金基体之间进行相互熔渗,导致PCBN层在距硬质合金10~20μm处Co含量达到最大值;PCBN的失效为穿晶断裂方式。